微波辐射法从茶叶中提取咖啡因工艺研究(附件)
摘 要 I
Abstract II
第1章 文献综述
1.1 引言 1
1.2 茶叶的概述 1
1.2.1 茶叶的来源 1
1.2.2 茶叶的分类 2
1.2.3 茶叶中含有的有效成分及其药理作用 2
1.3 咖啡因的概述 2
1.3.1 咖啡因的临床应用 2
1.3.2 咖啡因的物理、化学性质 2
1.4 提取咖啡因的国内外研究现状和发展趋势 3
1.5茶叶中咖啡因的提取方法 3
1.5.1传统提取法 3
1.5.1.1 水提法 4
1.5.1.2 升华法 4
1.5.1.3索氏提取法 4
1.5.1.4溶剂萃取法 5
1.5.2新型工艺及方法 5
1.5.2.1 树脂法 5
1.5.2.2 超声辅助提取法 6
1.5.2.3 超临界二氧化碳萃取法 7
1.5.2.4微波辅助提取法 7
1.6 选题目的和选
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升华法 4
1.5.1.3索氏提取法 4
1.5.1.4溶剂萃取法 5
1.5.2新型工艺及方法 5
1.5.2.1 树脂法 5
1.5.2.2 超声辅助提取法 6
1.5.2.3 超临界二氧化碳萃取法 7
1.5.2.4微波辅助提取法 7
1.6 选题目的和选题思路 8
第二章 实验
2.1实验仪器与实验试剂 9
2.1.1主要实验仪器 9
2.1.2实验试剂 9
2.2实验方法与实验结果讨论 10
2.2.1溶剂配比对茶叶中咖啡因提取率的影响 10
2.2.2微波温度对茶叶中咖啡因提取率的影响 10
2.2.3微波时间对茶叶中咖啡因提取率的影响 11
2.3响应曲面优化实验 12
2.3.1 响应面实验设计与结果 12
2.3.2任意两因素间的相互作用 14
2.4咖啡因标准曲线的绘制 15
2.5咖啡因含量的测定 16
结论 17
参考文献 18
致谢 20
Abstract
China tea culture broad and profound, from ancient heritage has been nearly a thousand years of history. From the initial to todays tea tea, tea from the direct consumption of specific parts of the original meet peoples demand for it now through processing, because tea contains complex composition, not only contains the energy and protein to maintain the function of the body of the normal operation of the material, but also contains a lot of has the pharmacological effects of alkaloids and other substances. Caffeine as a major alkaloid in tea, which has sedative, nerve paralysis and other central nervous excitement and effectiveness in the clinical application in the treatment of neurasthenia and impotent etc. due to the content less caffeine in plants, with the aging of society is becoming increasingly serious, the clinical demand of caffeine increases, cause caffeine insufficient supply of raw materials, making more and more The researchers focused their attention on increasing the yield of caffeine.
The microwave method extraction of caffeine from tea, and by study the proportion of different solvent, different feed liquid ratio, microwave radiation temperature and microwave radiation time effect on the extraction rate of determined the best scheme. On the basis of single factor experiment, and is verified by response surface method. Experimental results show that the tea caffeine solvent ratio, ratio of material to liquid6.5:1, microwave temperature for350, microwave time310s.Under the condition of extraction rate reached3.4%±0.5.
Key words: microwave method; tea ;caffeine; response surface method.
第1章 文献综述
1.1 引言
茶叶有着近千年的历史,由起初的饮品原料现越来越多的引用到其他方面。因为茶叶中有效成分多而复杂,不仅含有热能、矿物质和维生素等,还包含茶多酚、儿茶素及生物碱等多
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